Effect of cold sintering process (CSP) on the electro-chemo-mechanical properties of Gd-doped ceria (GDC)
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Effect of cold sintering process (CSP) on the electro-chemo-mechanical properties of Gd-doped ceria (GDC). / Kabir, Ahsanul; Espineira-Cachaza, Marti; Fiordaliso, Elisabetta Maria; Ke, Daoyao; Grasso, Salvatore; Merle, Benoit; Esposito, Vincenzo.
I: Journal of the European Ceramic Society, Bind 40, Nr. 15, 12.2020, s. 5612-5618.Publikation: Bidrag til tidsskrift › Tidsskriftartikel › Forskning › fagfællebedømt
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TY - JOUR
T1 - Effect of cold sintering process (CSP) on the electro-chemo-mechanical properties of Gd-doped ceria (GDC)
AU - Kabir, Ahsanul
AU - Espineira-Cachaza, Marti
AU - Fiordaliso, Elisabetta Maria
AU - Ke, Daoyao
AU - Grasso, Salvatore
AU - Merle, Benoit
AU - Esposito, Vincenzo
PY - 2020/12
Y1 - 2020/12
N2 - In this report, the effect of the cold sintering process (CSP) on the electro-chemo-mechanical properties of 10 mol % Gd-doped ceria (GDC) is investigated. High purity nanoscale GDC powder is sintered via a cold sintering process (CSP) in pure water followed by post-annealing at 1000 degrees C. The resultant ceramics exhibits high relative density (similar to 90 %) with a fine grain size of similar to 100 nm. This sample illustrates comparable electrochemical properties at intermediate-high temperatures and electromechanical properties at room temperature to the material prepared via conventional firing, i.e., sintering in the air at 1450 degrees C. Moreover, a large creep constant, as well a low elastic modulus and hardness, are also observed in the CSP sample.
AB - In this report, the effect of the cold sintering process (CSP) on the electro-chemo-mechanical properties of 10 mol % Gd-doped ceria (GDC) is investigated. High purity nanoscale GDC powder is sintered via a cold sintering process (CSP) in pure water followed by post-annealing at 1000 degrees C. The resultant ceramics exhibits high relative density (similar to 90 %) with a fine grain size of similar to 100 nm. This sample illustrates comparable electrochemical properties at intermediate-high temperatures and electromechanical properties at room temperature to the material prepared via conventional firing, i.e., sintering in the air at 1450 degrees C. Moreover, a large creep constant, as well a low elastic modulus and hardness, are also observed in the CSP sample.
KW - Gd-doped ceria
KW - Cold sintering
KW - Oxygen defects
KW - Creep
KW - Electrostriction
KW - STRAIN-RATE SENSITIVITY
KW - IONIC-CONDUCTIVITY
KW - ELASTIC-MODULUS
KW - LOW-TEMPERATURE
KW - GRAIN-GROWTH
KW - NANOINDENTATION
KW - DENSIFICATION
KW - INDENTATION
KW - MEMBRANES
KW - CERAMICS
U2 - 10.1016/j.jeurceramsoc.2020.06.010
DO - 10.1016/j.jeurceramsoc.2020.06.010
M3 - Journal article
VL - 40
SP - 5612
EP - 5618
JO - Journal of the European Ceramic Society
JF - Journal of the European Ceramic Society
SN - 0955-2219
IS - 15
ER -
ID: 248545350